------------------------------------------------------------------------------- -- -- -- Experiment Source Code -- -- Delta NMR Experiment & Machine Control Interface -- -- -- -- Copyright (c) 2000 JEOL Ltd -- -- All Rights Reserved -- -- -- ------------------------------------------------------------------------------- -- HELP.eng: spin echo -- Category: solids, spin echo, solids relaxation header filename => "RNTQ_2D"; sample_id => ""; comment => "RNTQ_2D"; process = "1d_solid.list"; include "header_solid"; end header; instrument include "instrument_solid"; end instrument; acquisition x_domain => "Proton"; x_offset => 5[ppm]; x_sweep => 100[kHz]; x_points => 1024; scans => 12; x_prescans => 0; mod_return => 1; y_domain = x_domain; y_offset = x_offset * 3; y_sweep => x_sweep; y_dwell =? 1/y_sweep; y_points => 24; include "acquisition_solid"; include "acquisition_2d"; end acquisition; pulse collect COMPLEX,OBS COMPLEX; initial_wait = 10.0[ms]; Pulse_Setup =? "-----------Setup hard pulses-----------"; obs_width_90 => x90, help "90deg pulse width"; obs_amp_pulse => 100[%], 0[%]->100[%]:0.01[%], help "ampliper"; irr_domain = x_domain; irr_offset = x_offset; RN_Setup =? "-----------Setup RN pulses-----------"; spinning_freq => 100 [kHz]; number_large_N => 12; number_n => 2; number_nu => 5; number_RN => 1; obs_amp_RN => 0[%]; obs_phs_RN_p = 180*number_nu/number_large_N; obs_phs_RN_m = -obs_phs_RN_p; obs_width_RN = (number_n/spinning_freq)/number_large_N; supercycle => "S0Sinv", ("S0","S0S180","S0Sinv","S0Sinv_180"); recoupling =? if supercycle = "S0" then number_RN*number_n/spinning_freq else if supercycle = "S0S180" then 2*number_RN*number_n/spinning_freq else if supercycle = "S0Sinv" then 2*number_RN*number_n/spinning_freq else if supercycle = "S0Sinv_180" then 4*number_RN*number_n/spinning_freq else 0[us]; z_filter => 100[us],0[ns] -> 50[ms] : 20[ns], help "total echo time"; MISC_Setup =? "-----------Setup Miscellaneous-----------"; relaxation_delay => 5.0[s], help "inter-pulse delay"; repetition_time =? relaxation_delay + x_acq_time, help "relaxation_delay+x_acq_time"; obs_atn => xatn, help "attenuator for x pulse"; obs_phs_exc = { 0..300:60, 30..330:60}.ystep(60%2); obs_phs_rec = { 0}; obs_phs_restore = {6( 0),6(120),6(240)}; obs_phs_acq = {3( 0,180),3(120,300),3(240, 60)}.ystep(180%2); include "pulse_solid"; module_config = "solid_sample"; begin initial_wait; relaxation_delay; loop number_RN times loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; when supercycle = "S0S180" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; when supercycle = "S0Sinv" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; when supercycle = "S0Sinv_180" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; end loop; loop number_RN times loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc+120), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc+120), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; when supercycle = "S0S180" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc+300), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc+300), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; when supercycle = "S0Sinv" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc-120), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc-120), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; when supercycle = "S0Sinv_180" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc-120), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc-120), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc+300), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc+300), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc+ 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc+ 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; end loop; loop number_RN times loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc+240), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc+240), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; when supercycle = "S0S180" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc+ 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc+ 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; when supercycle = "S0Sinv" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc-240), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc-240), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; when supercycle = "S0Sinv_180" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc-240), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc-240), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_exc- 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_exc- 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; end loop; 0[us] ystep 1/y_sweep; loop number_RN times loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; when supercycle = "S0S180" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; when supercycle = "S0Sinv" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; when supercycle = "S0Sinv_180" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec+180), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; end loop; loop number_RN times loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec+120), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec+120), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; when supercycle = "S0S180" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec+300), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec+300), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; when supercycle = "S0Sinv" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec-120), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec-120), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; when supercycle = "S0Sinv_180" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec-120), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec-120), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec+300), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec+300), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec+ 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec+ 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; end loop; loop number_RN times loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec+240), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec+240), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; when supercycle = "S0S180" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec+ 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec+ 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; when supercycle = "S0Sinv" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec-240), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec-240), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; when supercycle = "S0Sinv_180" do loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec-240), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec-240), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec+ 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec+ 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; loop number_large_N/2 times obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_m+obs_phs_rec- 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); obs_width_RN, (obs.gate, obs.phs.(obs_phs_RN_p+obs_phs_rec- 60), obs.amp.obs_amp_RN, obs.atn.obs_atn); end loop; end when; end loop; z_filter; obs_width_90, (obs.gate, obs.phs.obs_phs_restore, obs.amp.obs_amp_pulse, obs.atn.obs_atn); acq( dead_time, delay, obs_phs_acq ); end pulse;